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ARKIVOC Volume 2002
Part (xi): Commemorative Issue in Honor of Prof. Domenico Spinelli on the occasion of his 70th anniversary
Facilitator: Girolamo Cirrincione
Scientific Editor: Anthony Waring

Graphical Abstracts
1. A Tribute to Prof. Domenico Spinelli (MS-468HT)
Girolamo Cirrincione
DOI: https://doi.org/10.3998/ark.5550190.0003.b01
Full Text: PDF (171K)
pp. 1 - 5
accepted Oct 28 2002; published Nov 5 2002;
2. The conversion of furan-, thiophene- and selenophene-2-carbonyl azides into isocyanates: a DSC analysis (MS-373HP)
Elisabetta Salatelli and Paolo Zanirato
DOI: https://doi.org/10.3998/ark.5550190.0003.b02
Full Text: PDF (154K)
pp. 6 - 16
received Mar 22 2002; accepted Sep 19 2002; published Sep 27 2002;
3. Keto–enol interconversion of 2-phenacylfuran in aqueous solution and in the presence of surfactant micelles (MS-541HP)
Paolo De Maria, Antonella Fontana, Gabriella Siani, Antonio Arcadi and Marco Chiarini
DOI: https://doi.org/10.3998/ark.5550190.0003.b03
Full Text: PDF (157K)
pp. 17 - 31
received Jul 20 2002; accepted Nov 3 2002; published Nov 11 2002;
4. Cancer fighting cancer: synthesis of the new heterocyclic system diimidazo[1,2-a:1,2-c]pyrimidine (MS-561HP)
Aldo Andreani, Massimiliano Granaiola, Alberto Leoni, Alessandra Locatelli, Rita Morigi, Mirella Rambaldi, Gianluca Giorgi and Laura Salvini
DOI: https://doi.org/10.3998/ark.5550190.0003.b04
Full Text: PDF (186K)
pp. 32 - 38
received Sep 25 2002; accepted Nov 3 2002; published Nov 11 2002;
5. An efficient conversion of carboxylic acids into Weinreb amides (MS-553HP)
Alan R. Katritzky, Hongfang Yang, Suoming Zhang and Mingyi Wang
DOI: https://doi.org/10.3998/ark.5550190.0003.b05
Full Text: PDF (107K)
pp. 39 - 44
received Sep 11 2002; accepted Nov 15 2002; published Nov 23 2002;
6. Highly enantioselective reduction of ethyl 4-chloro-3-oxobutanoate to L- and D- 3-hydroxyesters with baker’s yeast (MS-566HP)
Arrigo Forni, Emilia Caselli, Fabio Prati, Maria Bucciarelli and Giovanni Torre
DOI: https://doi.org/10.3998/ark.5550190.0003.b06
Full Text: PDF (119K)
pp. 45 - 53
received Oct 4 2002; accepted Nov 15 2002; published Nov 23 2002;
7. Principal properties (PPs) as solvent descriptors for multivariate optimisation in organic synthesis: specific PPs for ethers (MS-568HP)
Francesco P. Ballistreri, Cosimo G. Fortuna, Giuseppe Musumarra, Didier Pavone and Salvatore Scirè
DOI: https://doi.org/10.3998/ark.5550190.0003.b07
Full Text: PDF (140K)
pp. 54 - 64
received Oct 7 2002; accepted Nov 21 2002; published Nov 29 2002;
8. The photochemical dimerization of 3-heteroaryl-acrylates (MS-575HR)
Maurizio D’Auria, Lucia Emanuele, Vittorio Esposito and Rocco Racioppi
DOI: https://doi.org/10.3998/ark.5550190.0003.b08
Full Text: PDF (166K)
pp. 65 - 78
received Oct 11 2002; accepted Nov 21 2002; published Nov 29 2002;
9. Synthesis and Diels-Alder reactivity of sulfinyl homo- and heterodienes obtained via enantiopure sulfenic acids (MS-579HP)
Maria C. Aversa, Anna Barattucci, Paola Bonaccorsi and Placido Giannetto
DOI: https://doi.org/10.3998/ark.5550190.0003.b09
Full Text: PDF (192K)
pp. 79 - 98
received Oct 16 2002; accepted Nov 24 2002; published Dec 2 2002;
10. Cyclic tetramers from 3,5-disubstituted 4-hydroxybenzenesulfonyl chlorides. A conformational study (MS-584HP)
Giorgio Cevasco, Fernando Sancassan and Sergio Thea
DOI: https://doi.org/10.3998/ark.5550190.0003.b10
Full Text: PDF (43K)
pp. 99 - 103
received Oct 18 2002; accepted Dec 4 2002; published Dec 12 2002;
11. Analysis of substituent effects in the reactions of some 2-L-3-nitro-5-X-thiophenes with aniline in benzene. A new interpretation of the ‘element effect’ (MS-581HP)
Giovanni Consiglio, Vincenzo Frenna, Susanna Guernelli and Gabriella Macaluso
DOI: https://doi.org/10.3998/ark.5550190.0003.b11
Full Text: PDF (150K)
pp. 104 - 117
received Oct 16 2002; accepted Dec 7 2002; published Dec 15 2002;
12. The formation of symmetrical glycosyl glycuronates by direct oxidation of partially protected methyl α-D-glycopyranosides (MS-576HP)
Giovanna Cupone, Antonio De Nino, Renato Dalpozzo, Loredana Maiuolo, Antonio Procopio and Giovanni Sindona
DOI: https://doi.org/10.3998/ark.5550190.0003.b12
Full Text: PDF (103K)
pp. 118 - 122
received Oct 13 2002; accepted Dec 7 2002; published Dec 15 2002;
13. Substituent effects on the formation of benzyl ions from ortho-methoxy substituted 1,1-diarylalkanes under electron ionization: correlations between the abundance of the process and the 13C-NMR chemical shifts of the neutral precursors (MS-577HP)
Leopoldo Ceraulo, Felice Filizzola, Gianfranco Fontana, Liliana Lamartina and Maria C. Natoli
DOI: https://doi.org/10.3998/ark.5550190.0003.b13
Full Text: PDF (257K)
pp. 123 - 141
received Oct 13 2002; accepted Dec 9 2002; published Dec 17 2002;
14. Access to 5,5'-diaryl substituted 4,5,4',5'-tetrahydro[3,3']bi-isoxazolyl 2,2'-dioxides, 4,5,4',5'-tetrahydro[3,3']bi-isoxazolyls and [3,3']bi-isoxazolyls via an initial ring-opening of 3,4-dinitrothiophene (MS-580HP)
Lara Bianchi, Carlo Dell’Erba, Francesco Gasparrini, Marino Novi, Giovanni Petrillo, Fernando Sancassan and Cinzia Tavani
DOI: https://doi.org/10.3998/ark.5550190.0003.b14
Full Text: PDF (264K)
pp. 142 - 158
received Oct 16 2002; accepted Dec 12 2002; published Dec 20 2002;
15. Enantioselective synthesis of isoxazolidinyl nucleosides containing uracil, 5-fluorouracil, thymine and cytosine as new potential anti-HIV drugs (MS-570HP)
Ugo Chiacchio, Antonino Corsaro, Daniela Iannazzo, Anna Piperno, Venerando Pistarà, Antonio Procopio, Antonio Rescifina, Giovanni Romeo, Roberto Romeo, Maria C. R. Siciliano and Enza Valveri
DOI: https://doi.org/10.3998/ark.5550190.0003.b15
Full Text: PDF (185K)
pp. 159 - 167
received Oct 8 2002; accepted Dec 11 2002; published Dec 19 2002;
16. The super-electrophilic reactivity of 4-nitro-6-trifluoromethanesulfonyl-benzofuroxan in aqueous solution (MS-593HP)
Malika Mokhtari, Régis Goumont, Jean Claude Hallé and François Terrier
DOI: https://doi.org/10.3998/ark.5550190.0003.b16
Full Text: PDF (133K)
pp. 168 - 186
received Oct 28 2002; accepted Dec 18 2002; published Dec 26 2002;
17. A kinetic study of the basic hydrolysis of 2-phenylethyl nitrite in the presence of borate buffer and β-cyclodextrin (MS-564HP)
Francesca D’Anna, M. Liria Turco Liveri and Renato Noto
DOI: https://doi.org/10.3998/ark.5550190.0003.b17
Full Text: PDF (235K)
pp. 187 - 197
received Oct 2 2002; accepted Dec 18 2002; published Dec 26 2002;
18. Reinvestigation of the tautomerism of some substituted 2-hydroxypyridines (MS-590HP)
Luciano Forlani, Giampiero Cristoni, Carla Boga, Paolo E. Todesco, Erminia Del Vecchio, Simona Selva and Magda Monari
DOI: https://doi.org/10.3998/ark.5550190.0003.b18
Full Text: PDF (320K)
pp. 198 - 215
received Oct 28 2002; accepted Dec 19 2002; published Dec 27 2002;
19. Regio- and stereo-selective coupling reactions of heteroarylalkyl propargyl ethers with electrophiles (MS-578HP)
Saverio Florio, Catia Granito, Giovanni Ingrosso and Luigino Troisi
DOI: https://doi.org/10.3998/ark.5550190.0003.b19
Full Text: PDF (71K)
pp. 216 - 226
received Oct 15 2002; accepted Dec 26 2002; published Jan 3 2003;
20. Synthesis of pyrazole-4-carbohydrazide derivatives of pharmaceutical interest (MS-588HP)
Giuseppe Daidone, Demetrio Raffa, Fabiana Plescia, Benedetta Maggio and Angela Roccaro
DOI: https://doi.org/10.3998/ark.5550190.0003.b20
Full Text: PDF (61K)
pp. 227 - 235
received Oct 23 2002; accepted Dec 26 2002; published Jan 3 2003;
21. Reactions of Fischer’s base with cyclic and acyclic conjugated nitroolefins and nitrovinylethers (MS-596HP)
Cristina Forzato, Fulvia Felluga, Patrizia Nitti, Giuliana Pitacco and Ennio Valentin
DOI: https://doi.org/10.3998/ark.5550190.0003.b21
Full Text: PDF (89K)
pp. 236 - 248
received Oct 30 2002; accepted Dec 31 2002; published Jan 8 2003;
22. Regioselective iodination of arenes in ionic liquids mediated by SelectfluorTM reagent F-TEDA-BF4 (MS-574HP)
Cinzia Chiappe and Daniela Pieraccini
DOI: https://doi.org/10.3998/ark.5550190.0003.b22
Full Text: PDF (112K)
pp. 249 - 255
received Oct 10 2002; accepted Jan 1 2003; published Jan 9 2003;
23. Synthesis, characterization and properties of a novel silicon-substituted soluble polymer with a PPV structure (MS-582HP)
Francesco Babudri, Gianluca M. Farinola, Omar Hassan Omar, Francesco Naso, Chiara Botta and Alberto Bolognesi
DOI: https://doi.org/10.3998/ark.5550190.0003.b23
Full Text: PDF (192K)
pp. 256 - 263
received Oct 18 2002; accepted Jan 14 2003; published Jan 22 2003;
24. Pyrimido[5,4-c]pyrrolo[2,1-a]isoquinoline: a new potential DNA-interactive ring system (MS-619HP)
Alessandra Montalbano, Patrizia Diana, Paola Barraja, Antonino Lauria, Girolamo Cirrincione, Gaetano Dattolo and Anna Maria Almerico
DOI: https://doi.org/10.3998/ark.5550190.0003.b24
Full Text: PDF (176K)
pp. 264 - 273
received Nov 29 2002; accepted Jan 14 2003; published Jan 22 2003;
25. 1,2-Diaza-1,3-butadienes: just a nice class of compounds, or powerful tools in organic chemistry? Reviewing an experience (MS-609HR)
Orazio A. Attanasi, Lucia De Crescentini, Paolino Filippone, Fabio Mantellini and Stefania Santeusanio
DOI: https://doi.org/10.3998/ark.5550190.0003.b25
Full Text: PDF (171K)
pp. 274 - 292
received Nov 18 2002; accepted Jan 20 2003; published Jan 28 2003;
26. Nucleophilic ring opening of 1,2-epoxides in aqueous medium (MS-573HR)
David Amantini, Francesco Fringuelli, Oriana Piermatti, Simone Tortoioli and Luigi Vaccaro
DOI: https://doi.org/10.3998/ark.5550190.0003.b26
Full Text: PDF (170K)
pp. 293 - 311
received Oct 10 2002; accepted Feb 28 2003; published Mar 8 2003;

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